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Beilstein J. Org. Chem. 2017, 13, 2854–2861, doi:10.3762/bjoc.13.277
Graphical Abstract
Scheme 1: Beirut reaction.
Scheme 2: Reactivity of 4,6-dinitrobenzofuroxan.
Scheme 3: Reactivity of ANBF (1).
Scheme 4: Synthesis of ANBF.
Scheme 5: Reactions of ANBF with β-dicarbonyl compounds.
Figure 1: General view of molecule 12 in crystal. Anisotropic displacement parameters for non-hydrogen atoms ...
Scheme 6: Reaction of ANBF with 2,4,6-trinitrotoluene.
Figure 2: Partial 1H NMR spectrum of compound 15 in DMSO-d6.
Figure 3: General view of molecule 15 in crystal. Anisotropic displacement parameters for non-hydrogen atoms ...
Scheme 7: Plausible mechanism of adducts formation.